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. 2013 Jan 18;6(3):537–544. doi: 10.1002/cssc.201200717

Table 2.

The BET surface area is calculated using the amount of N2 adsorbed at a relative vapour pressure of 0.06–0.35 at 77 K. Vtotal is the total pore volume determined at P/P0 of 0.99; Vmeso is the mesopore volume determined at P/P0 of 0.95; % mesopore volume is the percentage of the total pore volume that is mesoporous; 2r is the average pore diameter of the aerogels determined using the adsorption branch of the isotherm, using the BJH method

Initial chitin nanowhisker mass in gel [mg] BET surface area [m2 g−1] Vtotal [cm3 g−1] Vmeso [cm3 g−1] % mesopore volume 2r [nm]
40 116 0.34 0.21 62 % 13
50 177 0.49 0.31 63 % 13
60 126 0.33 0.23 70 % 12
70 212 0.64 0.40 63 % 14
70 194 0.66 0.37 56 % 15
80 177 0.69 0.37 54 % 17
80 190 0.64 0.37 58 % 14
90 58 0.19 0.11 58 % 15
100 198 0.60 0.37 62 % 14
100 261 0.75 0.48 64 % 12
120 125 0.47 0.25 53 % 17
120 212 0.68 0.43 63 % 13