Table 2.
The BET surface area is calculated using the amount of N2 adsorbed at a relative vapour pressure of 0.06–0.35 at 77 K. Vtotal is the total pore volume determined at P/P0 of 0.99; Vmeso is the mesopore volume determined at P/P0 of 0.95; % mesopore volume is the percentage of the total pore volume that is mesoporous; 2r is the average pore diameter of the aerogels determined using the adsorption branch of the isotherm, using the BJH method
Initial chitin nanowhisker mass in gel [mg] | BET surface area [m2 g−1] | Vtotal [cm3 g−1] | Vmeso [cm3 g−1] | % mesopore volume | 2r [nm] |
---|---|---|---|---|---|
40 | 116 | 0.34 | 0.21 | 62 % | 13 |
50 | 177 | 0.49 | 0.31 | 63 % | 13 |
60 | 126 | 0.33 | 0.23 | 70 % | 12 |
70 | 212 | 0.64 | 0.40 | 63 % | 14 |
70 | 194 | 0.66 | 0.37 | 56 % | 15 |
80 | 177 | 0.69 | 0.37 | 54 % | 17 |
80 | 190 | 0.64 | 0.37 | 58 % | 14 |
90 | 58 | 0.19 | 0.11 | 58 % | 15 |
100 | 198 | 0.60 | 0.37 | 62 % | 14 |
100 | 261 | 0.75 | 0.48 | 64 % | 12 |
120 | 125 | 0.47 | 0.25 | 53 % | 17 |
120 | 212 | 0.68 | 0.43 | 63 % | 13 |