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Summary of Validation Parameters for the Proposed Method
| Parameter | ASP | ATR |
|---|---|---|
| Linearitya (μg/mL) (n=3) | 1–80 | 1–60 |
| Intercept (c) | −21282 | −8019 |
| Slope (m) | 46251 | 36678 |
| r2 value | 0.999 | 0.999 |
| LOD (μg/mL) | 0.010 | 0.032 |
| LOQ (μg/mL) | 0.031 | 0.099 |
| Precision | ||
| Intraday % RSD (n=3) | 0.19–1.08 | 0.18–0.85 |
| Interday % RSD (n=3) | 0.03–0.5 | 0.15–042 |
| Repeatability % RSD (n=6) | 0.94 | 0.78 |
y = mx + c
