Table 1. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N1—H1C⋯O1 | 0.90 | 2.12 | 2.960 (3) | 155 |
| N1—H1D⋯Cl2 | 0.90 | 2.43 | 3.317 (2) | 170 |
| N2—H2C⋯Cl3i | 0.90 | 2.57 | 3.462 (2) | 172 |
| N2—H2D⋯Cl3 | 0.90 | 2.44 | 3.3196 (19) | 164 |
| N3—H3C⋯O1 | 0.90 | 2.04 | 2.880 (3) | 155 |
| N3—H3D⋯Cl3 | 0.90 | 2.50 | 3.3041 (18) | 149 |
| N4—H4C⋯Cl3ii | 0.90 | 2.65 | 3.486 (2) | 155 |
| N4—H4D⋯Cl2 | 0.90 | 2.45 | 3.348 (2) | 177 |
| N5—H5C⋯Cl3i | 0.90 | 2.49 | 3.359 (2) | 162 |
| N5—H5D⋯Cl3ii | 0.90 | 2.37 | 3.2649 (19) | 172 |
| O1—H1E⋯Cl2iii | 0.82 (4) | 2.29 (4) | 3.093 (3) | 168 (4) |
| O1—H1F⋯Cl2iv | 0.87 (4) | 2.25 (4) | 3.112 (3) | 174 (3) |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
.