| Oxford Diffraction XcaliburIII Sapphire-3 CCD diffractometer | 4874 independent reflections |
| Radiation source: fine-focus sealed tube | 3294 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.085 |
| Detector resolution: 16.5467 pixels mm-1 | θmax = 29.6°, θmin = 3.1° |
| ω scans at different φ | h = −9→8 |
| Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2007) | k = −27→28 |
| Tmin = 0.891, Tmax = 1.000 | l = −31→27 |
| 26916 measured reflections |