Skip to main content
. 2013 Mar 2;69(Pt 4):o467–o468. doi: 10.1107/S1600536813005606
Oxford Diffraction XcaliburIII Sapphire-3 CCD diffractometer 4874 independent reflections
Radiation source: fine-focus sealed tube 3294 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.085
Detector resolution: 16.5467 pixels mm-1 θmax = 29.6°, θmin = 3.1°
ω scans at different φ h = −9→8
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2007) k = −27→28
Tmin = 0.891, Tmax = 1.000 l = −31→27
26916 measured reflections