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. 2013 Mar 9;69(Pt 4):o527–o528. doi: 10.1107/S1600536813006326
Bruker Kappa APEXII DUO diffractometer 13651 independent reflections
Radiation source: IµS microfocus 13253 reflections with I > 2σ(I)
QUAZAR multilayer optics monochromator Rint = 0.028
φ and ω scans θmax = 68.1°, θmin = 4.6°
Absorption correction: multi-scan (SADABS; Sheldrick, 2004) h = −10→11
Tmin = 0.844, Tmax = 0.910 k = −6→12
26145 measured reflections l = −53→53