Bruker Kappa APEXII DUO diffractometer | 13651 independent reflections |
Radiation source: IµS microfocus | 13253 reflections with I > 2σ(I) |
QUAZAR multilayer optics monochromator | Rint = 0.028 |
φ and ω scans | θmax = 68.1°, θmin = 4.6° |
Absorption correction: multi-scan (SADABS; Sheldrick, 2004) | h = −10→11 |
Tmin = 0.844, Tmax = 0.910 | k = −6→12 |
26145 measured reflections | l = −53→53 |