| O1—C9 | 1.513 (3) | C3—H3A | 0.9700 |
| O1—C13 | 1.352 (3) | C3—H3B | 0.9700 |
| O2—C13 | 1.205 (3) | C4—H4A | 0.9700 |
| O3—C27 | 1.463 (4) | C4—H4B | 0.9700 |
| O3—C31 | 1.333 (5) | C6—H6 | 0.9800 |
| O4—C31 | 1.191 (6) | C7—H7 | 0.9800 |
| C1—C2 | 1.536 (5) | C8—H8A | 0.9600 |
| C2—C3 | 1.524 (4) | C8—H8B | 0.9600 |
| C2—C7 | 1.554 (4) | C8—H8C | 0.9600 |
| C3—C4 | 1.524 (5) | C11—H11A | 0.9700 |
| C4—C5 | 1.524 (4) | C11—H11B | 0.9700 |
| C5—C6 | 1.537 (4) | C12—H12A | 0.9700 |
| C5—C12 | 1.548 (4) | C12—H12B | 0.9700 |
| C5—C13 | 1.512 (4) | C14—H14A | 0.9600 |
| C6—C7 | 1.531 (4) | C14—H14B | 0.9600 |
| C6—C9 | 1.560 (3) | C14—H14C | 0.9600 |
| C7—C8 | 1.525 (4) | C16—H16 | 0.9800 |
| C9—C10 | 1.558 (3) | C17—H17 | 0.9300 |
| C9—C18 | 1.491 (3) | C18—H18 | 0.9300 |
| C10—C11 | 1.541 (3) | C19—H19A | 0.9600 |
| C10—C14 | 1.543 (4) | C19—H19B | 0.9600 |
| C10—C15 | 1.595 (3) | C19—H19C | 0.9600 |
| C11—C12 | 1.534 (4) | C20—H20A | 0.9700 |
| C15—C16 | 1.559 (3) | C20—H20B | 0.9700 |
| C15—C19 | 1.548 (3) | C21—H21A | 0.9700 |
| C15—C20 | 1.544 (4) | C21—H21B | 0.9700 |
| C16—C17 | 1.507 (4) | C22—H22 | 0.9800 |
| C16—C23 | 1.563 (4) | C24—H24A | 0.9600 |
| C17—C18 | 1.322 (4) | C24—H24B | 0.9600 |
| C20—C21 | 1.531 (4) | C24—H24C | 0.9600 |
| C21—C22 | 1.528 (4) | C25—H25A | 0.9700 |
| C22—C23 | 1.565 (4) | C25—H25B | 0.9700 |
| C22—C28 | 1.567 (4) | C26—H26A | 0.9700 |
| C23—C24 | 1.549 (4) | C26—H26B | 0.9700 |
| C23—C25 | 1.541 (4) | C27—H27 | 0.9800 |
| C25—C26 | 1.536 (4) | C29—H29A | 0.9600 |
| C26—C27 | 1.508 (5) | C29—H29B | 0.9600 |
| C27—C28 | 1.530 (5) | C29—H29C | 0.9600 |
| C28—C29 | 1.535 (5) | C30—H30A | 0.9600 |
| C28—C30 | 1.545 (5) | C30—H30B | 0.9600 |
| C31—C32 | 1.503 (5) | C30—H30C | 0.9600 |
| C1—H1A | 0.9600 | C32—H32A | 0.9600 |
| C1—H1B | 0.9600 | C32—H32B | 0.9600 |
| C1—H1C | 0.9600 | C32—H32C | 0.9600 |
| C2—H2 | 0.9800 | ||
| C9—O1—C13 | 109.9 (2) | C5—C6—H6 | 104.00 |
| C27—O3—C31 | 118.0 (3) | C7—C6—H6 | 104.00 |
| C1—C2—C3 | 109.8 (3) | C9—C6—H6 | 104.00 |
| C1—C2—C7 | 111.9 (3) | C2—C7—H7 | 109.00 |
| C3—C2—C7 | 111.7 (2) | C6—C7—H7 | 109.00 |
| C2—C3—C4 | 113.6 (3) | C8—C7—H7 | 109.00 |
| C3—C4—C5 | 110.4 (2) | C7—C8—H8A | 109.00 |
| C4—C5—C6 | 111.9 (2) | C7—C8—H8B | 110.00 |
| C4—C5—C12 | 113.4 (2) | C7—C8—H8C | 109.00 |
| C4—C5—C13 | 114.5 (2) | H8A—C8—H8B | 109.00 |
| C6—C5—C12 | 110.7 (2) | H8A—C8—H8C | 109.00 |
| C6—C5—C13 | 99.5 (2) | H8B—C8—H8C | 110.00 |
| C12—C5—C13 | 105.9 (2) | C10—C11—H11A | 109.00 |
| C5—C6—C7 | 114.4 (2) | C10—C11—H11B | 109.00 |
| C5—C6—C9 | 99.4 (2) | C12—C11—H11A | 109.00 |
| C7—C6—C9 | 127.5 (2) | C12—C11—H11B | 109.00 |
| C2—C7—C6 | 107.2 (2) | H11A—C11—H11B | 108.00 |
| C2—C7—C8 | 111.9 (2) | C5—C12—H12A | 109.00 |
| C6—C7—C8 | 111.8 (2) | C5—C12—H12B | 109.00 |
| O1—C9—C6 | 97.34 (18) | C11—C12—H12A | 109.00 |
| O1—C9—C10 | 107.66 (19) | C11—C12—H12B | 109.00 |
| O1—C9—C18 | 105.9 (2) | H12A—C12—H12B | 108.00 |
| C6—C9—C10 | 115.8 (2) | C10—C14—H14A | 109.00 |
| C6—C9—C18 | 115.9 (2) | C10—C14—H14B | 110.00 |
| C10—C9—C18 | 112.3 (2) | C10—C14—H14C | 109.00 |
| C9—C10—C11 | 108.7 (2) | H14A—C14—H14B | 109.00 |
| C9—C10—C14 | 109.2 (2) | H14A—C14—H14C | 109.00 |
| C9—C10—C15 | 109.1 (2) | H14B—C14—H14C | 109.00 |
| C11—C10—C14 | 107.0 (2) | C15—C16—H16 | 104.00 |
| C11—C10—C15 | 112.7 (2) | C17—C16—H16 | 104.00 |
| C14—C10—C15 | 110.1 (2) | C23—C16—H16 | 104.00 |
| C10—C11—C12 | 113.0 (2) | C16—C17—H17 | 118.00 |
| C5—C12—C11 | 112.5 (2) | C18—C17—H17 | 118.00 |
| O1—C13—O2 | 121.4 (3) | C9—C18—H18 | 118.00 |
| O1—C13—C5 | 109.0 (2) | C17—C18—H18 | 118.00 |
| O2—C13—C5 | 129.6 (3) | C15—C19—H19A | 109.00 |
| C10—C15—C16 | 106.72 (19) | C15—C19—H19B | 109.00 |
| C10—C15—C19 | 111.6 (2) | C15—C19—H19C | 110.00 |
| C10—C15—C20 | 111.6 (2) | H19A—C19—H19B | 109.00 |
| C16—C15—C19 | 111.2 (2) | H19A—C19—H19C | 110.00 |
| C16—C15—C20 | 109.0 (2) | H19B—C19—H19C | 109.00 |
| C19—C15—C20 | 106.7 (2) | C15—C20—H20A | 109.00 |
| C15—C16—C17 | 109.3 (2) | C15—C20—H20B | 109.00 |
| C15—C16—C23 | 117.36 (19) | C21—C20—H20A | 109.00 |
| C17—C16—C23 | 115.8 (2) | C21—C20—H20B | 109.00 |
| C16—C17—C18 | 124.6 (2) | H20A—C20—H20B | 108.00 |
| C9—C18—C17 | 124.0 (2) | C20—C21—H21A | 109.00 |
| C15—C20—C21 | 113.1 (2) | C20—C21—H21B | 109.00 |
| C20—C21—C22 | 111.6 (2) | C22—C21—H21A | 109.00 |
| C21—C22—C23 | 111.0 (2) | C22—C21—H21B | 109.00 |
| C21—C22—C28 | 114.2 (2) | H21A—C21—H21B | 108.00 |
| C23—C22—C28 | 117.5 (2) | C21—C22—H22 | 104.00 |
| C16—C23—C22 | 105.7 (2) | C23—C22—H22 | 104.00 |
| C16—C23—C24 | 112.3 (2) | C28—C22—H22 | 104.00 |
| C16—C23—C25 | 108.0 (2) | C23—C24—H24A | 109.00 |
| C22—C23—C24 | 115.5 (2) | C23—C24—H24B | 109.00 |
| C22—C23—C25 | 107.6 (2) | C23—C24—H24C | 109.00 |
| C24—C23—C25 | 107.5 (2) | H24A—C24—H24B | 109.00 |
| C23—C25—C26 | 112.6 (2) | H24A—C24—H24C | 110.00 |
| C25—C26—C27 | 110.7 (3) | H24B—C24—H24C | 109.00 |
| O3—C27—C26 | 108.4 (3) | C23—C25—H25A | 109.00 |
| O3—C27—C28 | 109.1 (3) | C23—C25—H25B | 109.00 |
| C26—C27—C28 | 115.0 (3) | C26—C25—H25A | 109.00 |
| C22—C28—C27 | 105.7 (2) | C26—C25—H25B | 109.00 |
| C22—C28—C29 | 114.1 (3) | H25A—C25—H25B | 108.00 |
| C22—C28—C30 | 108.7 (2) | C25—C26—H26A | 110.00 |
| C27—C28—C29 | 111.8 (3) | C25—C26—H26B | 110.00 |
| C27—C28—C30 | 107.9 (3) | C27—C26—H26A | 110.00 |
| C29—C28—C30 | 108.5 (3) | C27—C26—H26B | 110.00 |
| O3—C31—O4 | 123.7 (3) | H26A—C26—H26B | 108.00 |
| O3—C31—C32 | 111.1 (4) | O3—C27—H27 | 108.00 |
| O4—C31—C32 | 125.1 (4) | C26—C27—H27 | 108.00 |
| C2—C1—H1A | 109.00 | C28—C27—H27 | 108.00 |
| C2—C1—H1B | 109.00 | C28—C29—H29A | 109.00 |
| C2—C1—H1C | 109.00 | C28—C29—H29B | 110.00 |
| H1A—C1—H1B | 109.00 | C28—C29—H29C | 109.00 |
| H1A—C1—H1C | 109.00 | H29A—C29—H29B | 109.00 |
| H1B—C1—H1C | 110.00 | H29A—C29—H29C | 109.00 |
| C1—C2—H2 | 108.00 | H29B—C29—H29C | 110.00 |
| C3—C2—H2 | 108.00 | C28—C30—H30A | 109.00 |
| C7—C2—H2 | 108.00 | C28—C30—H30B | 109.00 |
| C2—C3—H3A | 109.00 | C28—C30—H30C | 109.00 |
| C2—C3—H3B | 109.00 | H30A—C30—H30B | 109.00 |
| C4—C3—H3A | 109.00 | H30A—C30—H30C | 109.00 |
| C4—C3—H3B | 109.00 | H30B—C30—H30C | 110.00 |
| H3A—C3—H3B | 108.00 | C31—C32—H32A | 109.00 |
| C3—C4—H4A | 110.00 | C31—C32—H32B | 110.00 |
| C3—C4—H4B | 110.00 | C31—C32—H32C | 109.00 |
| C5—C4—H4A | 110.00 | H32A—C32—H32B | 109.00 |
| C5—C4—H4B | 110.00 | H32A—C32—H32C | 109.00 |
| H4A—C4—H4B | 108.00 | H32B—C32—H32C | 109.00 |
| C13—O1—C9—C6 | −32.6 (2) | C14—C10—C11—C12 | 74.0 (3) |
| C13—O1—C9—C10 | 87.5 (2) | C15—C10—C11—C12 | −164.9 (2) |
| C13—O1—C9—C18 | −152.2 (2) | C9—C10—C15—C16 | 65.3 (2) |
| C9—O1—C13—O2 | −174.0 (2) | C9—C10—C15—C19 | −56.4 (3) |
| C9—O1—C13—C5 | 4.4 (3) | C9—C10—C15—C20 | −175.7 (2) |
| C31—O3—C27—C26 | 97.1 (4) | C11—C10—C15—C16 | −174.0 (2) |
| C31—O3—C27—C28 | −136.9 (3) | C11—C10—C15—C19 | 64.3 (3) |
| C27—O3—C31—O4 | 6.1 (6) | C11—C10—C15—C20 | −55.0 (3) |
| C27—O3—C31—C32 | −174.5 (3) | C14—C10—C15—C16 | −54.5 (2) |
| C1—C2—C3—C4 | 178.3 (2) | C14—C10—C15—C19 | −176.2 (2) |
| C7—C2—C3—C4 | −57.0 (3) | C14—C10—C15—C20 | 64.5 (3) |
| C1—C2—C7—C6 | 179.0 (2) | C10—C11—C12—C5 | 48.1 (3) |
| C1—C2—C7—C8 | −58.1 (3) | C10—C15—C16—C17 | −54.2 (3) |
| C3—C2—C7—C6 | 55.5 (3) | C10—C15—C16—C23 | 171.3 (2) |
| C3—C2—C7—C8 | 178.4 (3) | C19—C15—C16—C17 | 67.8 (3) |
| C2—C3—C4—C5 | 53.2 (3) | C19—C15—C16—C23 | −66.7 (3) |
| C3—C4—C5—C6 | −50.6 (3) | C20—C15—C16—C17 | −174.9 (2) |
| C3—C4—C5—C12 | 75.5 (3) | C20—C15—C16—C23 | 50.6 (3) |
| C3—C4—C5—C13 | −162.9 (2) | C10—C15—C20—C21 | −166.3 (2) |
| C4—C5—C6—C7 | 54.9 (3) | C16—C15—C20—C21 | −48.6 (3) |
| C4—C5—C6—C9 | −166.2 (2) | C19—C15—C20—C21 | 71.5 (3) |
| C12—C5—C6—C7 | −72.7 (3) | C15—C16—C17—C18 | 24.5 (4) |
| C12—C5—C6—C9 | 66.2 (3) | C23—C16—C17—C18 | 159.8 (3) |
| C13—C5—C6—C7 | 176.2 (2) | C15—C16—C23—C22 | −54.8 (3) |
| C13—C5—C6—C9 | −44.9 (2) | C15—C16—C23—C24 | 72.0 (3) |
| C4—C5—C12—C11 | 170.9 (2) | C15—C16—C23—C25 | −169.7 (2) |
| C6—C5—C12—C11 | −62.3 (3) | C17—C16—C23—C22 | 173.7 (2) |
| C13—C5—C12—C11 | 44.6 (3) | C17—C16—C23—C24 | −59.6 (3) |
| C4—C5—C13—O1 | 145.8 (2) | C17—C16—C23—C25 | 58.7 (3) |
| C4—C5—C13—O2 | −36.0 (4) | C16—C17—C18—C9 | −1.6 (5) |
| C6—C5—C13—O1 | 26.3 (3) | C15—C20—C21—C22 | 56.5 (3) |
| C6—C5—C13—O2 | −155.5 (3) | C20—C21—C22—C23 | −61.7 (3) |
| C12—C5—C13—O1 | −88.5 (2) | C20—C21—C22—C28 | 162.7 (2) |
| C12—C5—C13—O2 | 89.7 (3) | C21—C22—C23—C16 | 57.9 (3) |
| C5—C6—C7—C2 | −55.5 (3) | C21—C22—C23—C24 | −66.9 (3) |
| C5—C6—C7—C8 | −178.5 (2) | C21—C22—C23—C25 | 173.1 (2) |
| C9—C6—C7—C2 | 179.4 (2) | C28—C22—C23—C16 | −168.1 (2) |
| C9—C6—C7—C8 | 56.4 (3) | C28—C22—C23—C24 | 67.1 (3) |
| C5—C6—C9—O1 | 46.7 (2) | C28—C22—C23—C25 | −52.9 (3) |
| C5—C6—C9—C10 | −67.0 (3) | C21—C22—C28—C27 | −175.0 (3) |
| C5—C6—C9—C18 | 158.3 (2) | C21—C22—C28—C29 | 61.8 (3) |
| C7—C6—C9—O1 | 177.7 (2) | C21—C22—C28—C30 | −59.4 (4) |
| C7—C6—C9—C10 | 64.0 (3) | C23—C22—C28—C27 | 52.4 (3) |
| C7—C6—C9—C18 | −70.7 (3) | C23—C22—C28—C29 | −70.8 (3) |
| O1—C9—C10—C11 | −50.0 (3) | C23—C22—C28—C30 | 168.0 (3) |
| O1—C9—C10—C14 | −166.42 (19) | C16—C23—C25—C26 | 166.3 (3) |
| O1—C9—C10—C15 | 73.2 (2) | C22—C23—C25—C26 | 52.6 (3) |
| C6—C9—C10—C11 | 57.6 (3) | C24—C23—C25—C26 | −72.4 (3) |
| C6—C9—C10—C14 | −58.8 (3) | C23—C25—C26—C27 | −57.1 (4) |
| C6—C9—C10—C15 | −179.2 (2) | C25—C26—C27—O3 | −178.5 (3) |
| C18—C9—C10—C11 | −166.2 (2) | C25—C26—C27—C28 | 59.0 (4) |
| C18—C9—C10—C14 | 77.4 (3) | O3—C27—C28—C22 | −176.2 (2) |
| C18—C9—C10—C15 | −42.9 (3) | O3—C27—C28—C29 | −51.5 (3) |
| O1—C9—C18—C17 | −105.8 (3) | O3—C27—C28—C30 | 67.7 (3) |
| C6—C9—C18—C17 | 147.6 (3) | C26—C27—C28—C22 | −54.1 (3) |
| C10—C9—C18—C17 | 11.5 (4) | C26—C27—C28—C29 | 70.5 (3) |
| C9—C10—C11—C12 | −43.9 (3) | C26—C27—C28—C30 | −170.2 (3) |