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. 2013 Mar 28;69(Pt 4):o620. doi: 10.1107/S1600536813007976
Bruker X8 Proteum diffractometer 6651 independent reflections
Radiation source: fine-focus rotating anode 6238 reflections with I > 2σ(I)
Graded multilayer optics monochromator Rint = 0.062
Detector resolution: 5.6 pixels mm-1 θmax = 68.4°, θmin = 3.1°
φ and ω scans h = −14→16
Absorption correction: multi-scan (SADABS; Bruker, 2006) k = −10→11
Tmin = 0.504, Tmax = 0.830 l = −34→34
45894 measured reflections