Bruker X8 Proteum diffractometer | 6651 independent reflections |
Radiation source: fine-focus rotating anode | 6238 reflections with I > 2σ(I) |
Graded multilayer optics monochromator | Rint = 0.062 |
Detector resolution: 5.6 pixels mm-1 | θmax = 68.4°, θmin = 3.1° |
φ and ω scans | h = −14→16 |
Absorption correction: multi-scan (SADABS; Bruker, 2006) | k = −10→11 |
Tmin = 0.504, Tmax = 0.830 | l = −34→34 |
45894 measured reflections |