TABLE 1.
Experiment | Field | SWa | Offsetb | No. of experiments | No. of scans/experiment | Mixing time |
---|---|---|---|---|---|---|
MHz | ppm (Hz) | ppm | ms | |||
COSY | 600 | 5.32 (3193) | 3.65 | 1024 | 32 | |
TOCSY | 600 | 5.32 (3193) | 3.65 | 512 | 32 | 180 |
ROESY | 600 | 8.33 (5000) | 4.67 | 1024 | 56 | 350 |
TOCSY | 800 | 8.75 (7002) | 4.67 | 1024 | 24 | 180 |
ROESY | 800 | 11.24 (8992) | 5.91 | 1024 | 16 | 350 |
a SW, spectral width in both dimensions.
b Transmitter offset.