TABLE 4.

WIC29.26 epitope inter-residue ROEs

The chemical shifts of each ROESY cross-peak (H-1 and H-2) are given in ppm. The numbering of the ROEs corresponds to those indicated in Fig. 2. Me denotes the methyl protons of Fuc and Rha.

ROE number	H-1	Assignment			H-2	Assignment			ROE strength
		Sugar	Label	H		Sugar	Label	H
1	5.09	Galf	A	H1	3.50	Rha	B	H4	Strong
2	5.09	Galf	A	H1	1.31	Rha	B	Me	Weak
3	4.91	Rha	B	H1	5.19	Fuc	C	H1	Strong
4	4.91	Rha	B	H1	3.90	Fuc	C	H2	Strong
5	4.91	Rha	B	H1	3.95	Fuc	C	H3	Weak
6	5.19	Fuc	C	H1	4.19	Xyl	D	H5e	Weak
7	5.19	Fuc	C	H1	3.87	Xyl	D	H4	Strong
8	4.59	Fuc	C	H5	3.50	Xyl	D	H5a	Medium
9	5.46	Galp	E	H1	4.82	Xyl	D	H1	Weak
10	5.46	Galp	E	H1	3.79	Xyl	D	H2	Medium
11	4.68	Galp	F	H1	4.15	Xyl	D	H3	Medium
12	4.68	Galp	F	H1	3.85	Xyl	D	H4	Medium
13	4.68	Galp	F	H1	3.79	Xyl	D	H2	Weak
14	4.82	Xyl	D	H1	3.93	Xyl	G	H4	Weak
15	4.82	Xyl	D	H1	4.15	Xyl	Ga	H5e	Strong
16	4.48	Xyl	G	H1	4.06	GlcNac	H	H3	Strong
17	4.44	Xyl	K	H1	5.31	Galp	M	H1	Strong
18	4.44	Xyl	K	H1	4.32	Galp	M	H2	Strong
19	5.31	Galp	M	H1	3.92	Fuc	J	H4	Medium
20	5.31	Galp	M	H1	3.86	a			Medium
21	4.62	Fuc	J	H5	3.18	Xyl	G	H2	Medium
22	1.29	Rha	L	Me	5.08	Fuc	J	H1	Medium
23	4.71	Galp	N	H1	4.13	Fuc	J	H3	Medium

^a Ambiguous.