Table 3.
Hydrolysis of cyclohexanone-derived bisperoxyacetal 4
| |||
|---|---|---|---|
| solvent | temp | time (h) | yield |
| MeOH | reflux | 0.25 | 21% |
| THF | 50–55 °C | 6 | 34%a |
a
NMR-based yield
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