Table 2.
13C-NMR data of compounds 1–5 in ppm
COMPOUNDS | |||||
---|---|---|---|---|---|
Carbon |
1a |
2b |
3c |
4d |
5d |
1 |
155.0 |
154.9 |
158.1 |
157.6 |
158.2 |
2 |
128.0 |
128.0 |
127.8 |
127.9 |
127.7 |
3 |
185.8 |
185.8 |
188.7 |
188.6 |
188.7 |
4 |
122.9 |
122.9 |
122.7 |
122.8 |
122.7 |
5 |
167.9 |
167.9 |
171.6 |
171.2 |
171.7 |
6 |
147.1 |
147.0 |
147.7 |
147.3 |
147.8 |
7 |
39.87 |
32.1 |
41.4 |
41.2 |
41.3 |
8 |
36.0 |
39.6 |
36.6 |
35.9 |
37.2 |
9 |
50.9 |
48.6 |
51.9 |
51.4 |
51.7 |
10 |
44.3 |
44.3 |
45.6 |
45.5 |
45.6 |
11 |
22.63 |
71.5 |
23.0 |
23.2 |
23.6 |
12 |
32.0 |
32.0 |
38.1 |
36.6 |
37.5 |
13 |
48.1 |
48.1 |
43.7 |
43.5 |
44.2 |
14 |
51.3 |
50.8 |
48.2 |
45.4 |
51.8 |
15 |
22.3 |
22.3 |
35.9 |
36.6 |
24.3 |
16 |
35.8 |
39.7 |
70.6 |
217.7 |
30.5 |
17 |
218.8 |
218.0 |
81.7 |
86.8 |
82.1 |
18 |
13.9 |
14.5 |
12.5 |
11.9 |
11.6 |
19 |
20.1 |
20.1 |
20.1 |
20.1 |
20.1 |
20 | 112.2 | 112.2 | 112.6 | 112.9 | 112.4 |
a 125 MHz (CD3)2CO.
b 150 MHz (CD3)2CO.
c 125 MHz CD3OD.
d 75 MHz CD3OD.