Table 1. Data-collection and refinement statistics for Deg5 (S266A) and Deg8 (S292A).
| Deg5 (S266A) | Deg8 (S292A) | |
|---|---|---|
| Data collection | ||
| Space group | C2 | C2 |
| Unit-cell parameters (Å, °) | a = 109.1, b = 126.0, c = 83.3, β = 102.9 | a = 129.5, b = 124.2, c = 93.3, β = 132.4 |
| Resolution range (Å) | 50–2.6 (2.69–2.60) | 50–2.0 (2.07–2.00) |
| No. of reflections (total/unique) | 33072/11024 | 73478/9929 |
| 〈I/σ(I)〉 | 10.9 (2.3) | 25.2 (4.3) |
| Completeness (%) | 99.2 (97.8) | 99.3 (100.0) |
| Multiplicity (%) | 3.0 (2.9) | 7.4 (7.7) |
| Wilson B factor (Å2) | 50.2 | 37.5 |
| R merge (%) | 9.4 (46.5) | 6.7 (47.8) |
| Structure refinement | ||
| Resolution (Å) | 80–2.6 | 30–2.0 |
| R work | 0.182 | 0.198 |
| R free | 0.231 | 0.235 |
| Ramachandran plot (%) | ||
| Favoured region | 93.1 | 96.4 |
| Allowed region | 6.1 | 3.4 |
| Outlier region | 0.8 | 0.2 |
| R.m.s.d. bonds (Å) | 0.007 | 0.007 |
| R.m.s.d. angles (°) | 1.026 | 1.122 |
| Mean B value (Å2) | 51.7 | 51.8 |