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Influence of A) reaction temperature, B) hydrogen pressure, C) DTT concentration and D) pH value applied in the in situ protocol on yields and e.r. values achieved in the OMEH-catalyzed hydrogenation of 2,2,2-trifluoroacetophenone. If not specified otherwise, reaction conditions were as in Table 1, Entry 1. In A), a DTT concentration of 3.8 mM was used.
