Si1—O1 | 1.6464 (15) | C9—H9B | 0.9800 |
Si1—C9 | 1.863 (2) | C9—H9C | 0.9800 |
Si1—C8 | 1.864 (3) | C10—C12 | 1.527 (3) |
Si1—C10 | 1.874 (3) | C10—C11 | 1.544 (3) |
Si2—O5 | 1.6421 (16) | C10—C13 | 1.549 (3) |
Si2—C16 | 1.860 (2) | C11—H11A | 0.9800 |
Si2—C17 | 1.864 (2) | C11—H11B | 0.9800 |
Si2—C18 | 1.877 (3) | C11—H11C | 0.9800 |
O1—C1 | 1.427 (2) | C12—H12A | 0.9800 |
O2—C6 | 1.422 (2) | C12—H12B | 0.9800 |
O2—C7 | 1.435 (3) | C12—H12C | 0.9800 |
O3—C14 | 1.207 (3) | C13—H13A | 0.9800 |
O4—C14 | 1.347 (3) | C13—H13B | 0.9800 |
O4—C15 | 1.454 (3) | C13—H13C | 0.9800 |
O5—C5 | 1.440 (2) | C15—H15A | 0.9800 |
C1—C6 | 1.523 (3) | C15—H15B | 0.9800 |
C1—C2 | 1.530 (3) | C15—H15C | 0.9800 |
C1—H1 | 1.0000 | C16—H16A | 0.9800 |
C2—C3 | 1.513 (3) | C16—H16B | 0.9800 |
C2—H2A | 0.9900 | C16—H16C | 0.9800 |
C2—H2B | 0.9900 | C17—H17A | 0.9800 |
C3—C4 | 1.324 (3) | C17—H17B | 0.9800 |
C3—C14 | 1.475 (3) | C17—H17C | 0.9800 |
C4—C5 | 1.492 (3) | C18—C19 | 1.529 (3) |
C4—H4 | 0.9500 | C18—C20 | 1.536 (3) |
C5—C6 | 1.527 (3) | C18—C21 | 1.537 (3) |
C5—H5 | 1.0000 | C19—H19A | 0.9800 |
C6—H6 | 1.0000 | C19—H19B | 0.9800 |
C7—H7A | 0.9800 | C19—H19C | 0.9800 |
C7—H7B | 0.9800 | C20—H20A | 0.9800 |
C7—H7C | 0.9800 | C20—H20B | 0.9800 |
C8—H8A | 0.9800 | C20—H20C | 0.9800 |
C8—H8B | 0.9800 | C21—H21A | 0.9800 |
C8—H8C | 0.9800 | C21—H21B | 0.9800 |
C9—H9A | 0.9800 | C21—H21C | 0.9800 |
O1—Si1—C9 | 110.29 (10) | C12—C10—Si1 | 110.67 (18) |
O1—Si1—C8 | 110.58 (10) | C11—C10—Si1 | 109.69 (17) |
C9—Si1—C8 | 108.63 (12) | C13—C10—Si1 | 110.70 (16) |
O1—Si1—C10 | 103.74 (10) | C10—C11—H11A | 109.5 |
C9—Si1—C10 | 111.85 (11) | C10—C11—H11B | 109.5 |
C8—Si1—C10 | 111.69 (12) | H11A—C11—H11B | 109.5 |
O5—Si2—C16 | 108.88 (10) | C10—C11—H11C | 109.5 |
O5—Si2—C17 | 109.77 (10) | H11A—C11—H11C | 109.5 |
C16—Si2—C17 | 109.45 (12) | H11B—C11—H11C | 109.5 |
O5—Si2—C18 | 104.99 (10) | C10—C12—H12A | 109.5 |
C16—Si2—C18 | 111.41 (12) | C10—C12—H12B | 109.5 |
C17—Si2—C18 | 112.21 (11) | H12A—C12—H12B | 109.5 |
C1—O1—Si1 | 126.87 (15) | C10—C12—H12C | 109.5 |
C6—O2—C7 | 114.49 (18) | H12A—C12—H12C | 109.5 |
C14—O4—C15 | 115.5 (2) | H12B—C12—H12C | 109.5 |
C5—O5—Si2 | 122.79 (13) | C10—C13—H13A | 109.5 |
O1—C1—C6 | 108.68 (18) | C10—C13—H13B | 109.5 |
O1—C1—C2 | 108.40 (18) | H13A—C13—H13B | 109.5 |
C6—C1—C2 | 110.27 (18) | C10—C13—H13C | 109.5 |
O1—C1—H1 | 109.8 | H13A—C13—H13C | 109.5 |
C6—C1—H1 | 109.8 | H13B—C13—H13C | 109.5 |
C2—C1—H1 | 109.8 | O3—C14—O4 | 123.3 (2) |
C3—C2—C1 | 111.65 (19) | O3—C14—C3 | 124.1 (2) |
C3—C2—H2A | 109.3 | O4—C14—C3 | 112.5 (2) |
C1—C2—H2A | 109.3 | O4—C15—H15A | 109.5 |
C3—C2—H2B | 109.3 | O4—C15—H15B | 109.5 |
C1—C2—H2B | 109.3 | H15A—C15—H15B | 109.5 |
H2A—C2—H2B | 108.0 | O4—C15—H15C | 109.5 |
C4—C3—C14 | 122.0 (2) | H15A—C15—H15C | 109.5 |
C4—C3—C2 | 122.4 (2) | H15B—C15—H15C | 109.5 |
C14—C3—C2 | 115.5 (2) | Si2—C16—H16A | 109.5 |
C3—C4—C5 | 124.0 (2) | Si2—C16—H16B | 109.5 |
C3—C4—H4 | 118.0 | H16A—C16—H16B | 109.5 |
C5—C4—H4 | 118.0 | Si2—C16—H16C | 109.5 |
O5—C5—C4 | 110.08 (18) | H16A—C16—H16C | 109.5 |
O5—C5—C6 | 109.77 (18) | H16B—C16—H16C | 109.5 |
C4—C5—C6 | 111.52 (19) | Si2—C17—H17A | 109.5 |
O5—C5—H5 | 108.5 | Si2—C17—H17B | 109.5 |
C4—C5—H5 | 108.5 | H17A—C17—H17B | 109.5 |
C6—C5—H5 | 108.5 | Si2—C17—H17C | 109.5 |
O2—C6—C1 | 105.72 (18) | H17A—C17—H17C | 109.5 |
O2—C6—C5 | 111.78 (18) | H17B—C17—H17C | 109.5 |
C1—C6—C5 | 108.40 (19) | C19—C18—C20 | 109.1 (2) |
O2—C6—H6 | 110.3 | C19—C18—C21 | 109.3 (2) |
C1—C6—H6 | 110.3 | C20—C18—C21 | 108.9 (2) |
C5—C6—H6 | 110.3 | C19—C18—Si2 | 110.14 (17) |
O2—C7—H7A | 109.5 | C20—C18—Si2 | 108.56 (18) |
O2—C7—H7B | 109.5 | C21—C18—Si2 | 110.82 (16) |
H7A—C7—H7B | 109.5 | C18—C19—H19A | 109.5 |
O2—C7—H7C | 109.5 | C18—C19—H19B | 109.5 |
H7A—C7—H7C | 109.5 | H19A—C19—H19B | 109.5 |
H7B—C7—H7C | 109.5 | C18—C19—H19C | 109.5 |
Si1—C8—H8A | 109.5 | H19A—C19—H19C | 109.5 |
Si1—C8—H8B | 109.5 | H19B—C19—H19C | 109.5 |
H8A—C8—H8B | 109.5 | C18—C20—H20A | 109.5 |
Si1—C8—H8C | 109.5 | C18—C20—H20B | 109.5 |
H8A—C8—H8C | 109.5 | H20A—C20—H20B | 109.5 |
H8B—C8—H8C | 109.5 | C18—C20—H20C | 109.5 |
Si1—C9—H9A | 109.5 | H20A—C20—H20C | 109.5 |
Si1—C9—H9B | 109.5 | H20B—C20—H20C | 109.5 |
H9A—C9—H9B | 109.5 | C18—C21—H21A | 109.5 |
Si1—C9—H9C | 109.5 | C18—C21—H21B | 109.5 |
H9A—C9—H9C | 109.5 | H21A—C21—H21B | 109.5 |
H9B—C9—H9C | 109.5 | C18—C21—H21C | 109.5 |
C12—C10—C11 | 109.4 (2) | H21A—C21—H21C | 109.5 |
C12—C10—C13 | 108.7 (2) | H21B—C21—H21C | 109.5 |
C11—C10—C13 | 107.5 (2) | ||
C9—Si1—O1—C1 | 65.82 (19) | O5—C5—C6—C1 | 171.87 (16) |
C8—Si1—O1—C1 | −54.4 (2) | C4—C5—C6—C1 | 49.6 (2) |
C10—Si1—O1—C1 | −174.24 (17) | O1—Si1—C10—C12 | −70.14 (19) |
C16—Si2—O5—C5 | 63.48 (18) | C9—Si1—C10—C12 | 48.7 (2) |
C17—Si2—O5—C5 | −56.31 (18) | C8—Si1—C10—C12 | 170.72 (18) |
C18—Si2—O5—C5 | −177.12 (16) | O1—Si1—C10—C11 | 169.01 (16) |
Si1—O1—C1—C6 | 97.0 (2) | C9—Si1—C10—C11 | −72.1 (2) |
Si1—O1—C1—C2 | −143.19 (15) | C8—Si1—C10—C11 | 49.9 (2) |
O1—C1—C2—C3 | −73.1 (2) | O1—Si1—C10—C13 | 50.48 (19) |
C6—C1—C2—C3 | 45.8 (3) | C9—Si1—C10—C13 | 169.35 (17) |
C1—C2—C3—C4 | −13.4 (3) | C8—Si1—C10—C13 | −68.6 (2) |
C1—C2—C3—C14 | 170.15 (18) | C15—O4—C14—O3 | 2.6 (3) |
C14—C3—C4—C5 | 175.70 (19) | C15—O4—C14—C3 | −175.76 (18) |
C2—C3—C4—C5 | −0.5 (3) | C4—C3—C14—O3 | −170.6 (2) |
Si2—O5—C5—C4 | −110.40 (18) | C2—C3—C14—O3 | 5.9 (3) |
Si2—O5—C5—C6 | 126.48 (16) | C4—C3—C14—O4 | 7.8 (3) |
C3—C4—C5—O5 | −140.3 (2) | C2—C3—C14—O4 | −175.7 (2) |
C3—C4—C5—C6 | −18.3 (3) | O5—Si2—C18—C19 | −43.92 (18) |
C7—O2—C6—C1 | 151.68 (18) | C16—Si2—C18—C19 | 73.8 (2) |
C7—O2—C6—C5 | −90.6 (2) | C17—Si2—C18—C19 | −163.11 (17) |
O1—C1—C6—O2 | 173.92 (17) | O5—Si2—C18—C20 | −163.30 (16) |
C2—C1—C6—O2 | 55.2 (2) | C16—Si2—C18—C20 | −45.6 (2) |
O1—C1—C6—C5 | 53.9 (2) | C17—Si2—C18—C20 | 77.52 (19) |
C2—C1—C6—C5 | −64.8 (2) | O5—Si2—C18—C21 | 77.13 (18) |
O5—C5—C6—O2 | 55.7 (2) | C16—Si2—C18—C21 | −165.17 (17) |
C4—C5—C6—O2 | −66.5 (2) | C17—Si2—C18—C21 | −42.1 (2) |