Rigaku Saturn724 CCD diffractometer | 6015 independent reflections |
Radiation source: rotating anode | 4456 reflections with I > 2σ(I) |
Multilayer monochromator | Rint = 0.058 |
Detector resolution: 14.22 pixels mm-1 | θmax = 27.9°, θmin = 1.9° |
ω and φ scans | h = −14→14 |
Absorption correction: multi-scan (CrystalClear; Rigaku, 2007) | k = −10→10 |
Tmin = 0.968, Tmax = 0.981 | l = −19→19 |
13589 measured reflections |