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. 2013 Apr 5;69(Pt 5):o632. doi: 10.1107/S1600536813007551
Rigaku Saturn724 CCD diffractometer 6015 independent reflections
Radiation source: rotating anode 4456 reflections with I > 2σ(I)
Multilayer monochromator Rint = 0.058
Detector resolution: 14.22 pixels mm-1 θmax = 27.9°, θmin = 1.9°
ω and φ scans h = −14→14
Absorption correction: multi-scan (CrystalClear; Rigaku, 2007) k = −10→10
Tmin = 0.968, Tmax = 0.981 l = −19→19
13589 measured reflections