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. 2013 Apr 5;69(Pt 5):o632. doi: 10.1107/S1600536813007551
x y z Uiso*/Ueq
Si1 0.43693 (6) 0.59832 (8) 0.75544 (5) 0.02755 (16)
Si2 0.93837 (6) 0.92816 (8) 0.82849 (4) 0.02554 (16)
O1 0.55081 (13) 0.59788 (19) 0.69212 (10) 0.0277 (4)
O2 0.66743 (13) 0.92780 (19) 0.57018 (10) 0.0307 (4)
O3 0.75863 (16) 0.3984 (2) 0.44370 (12) 0.0421 (5)
O4 0.93371 (15) 0.4208 (2) 0.54942 (11) 0.0367 (4)
O5 0.86351 (13) 0.89726 (17) 0.72306 (10) 0.0246 (4)
C1 0.5623 (2) 0.7011 (3) 0.61583 (16) 0.0274 (6)
H1 0.4777 0.7436 0.5885 0.033*
C2 0.61777 (19) 0.6039 (3) 0.54295 (15) 0.0290 (5)
H2A 0.5717 0.5011 0.5319 0.035*
H2B 0.6066 0.6644 0.4838 0.035*
C3 0.7562 (2) 0.5697 (3) 0.57327 (15) 0.0250 (5)
C4 0.8238 (2) 0.6447 (3) 0.64413 (15) 0.0238 (5)
H4 0.9101 0.6167 0.6598 0.029*
C5 0.7728 (2) 0.7704 (3) 0.70088 (15) 0.0242 (5)
H5 0.7564 0.7202 0.7601 0.029*
C6 0.6494 (2) 0.8400 (3) 0.65060 (15) 0.0266 (6)
H6 0.6093 0.9098 0.6935 0.032*
C7 0.6928 (2) 1.0957 (3) 0.58602 (16) 0.0488 (7)
H7A 0.6265 1.1434 0.6163 0.073*
H7B 0.6950 1.1496 0.5266 0.073*
H7C 0.7743 1.1086 0.6260 0.073*
C8 0.4174 (2) 0.8026 (3) 0.80365 (17) 0.0441 (7)
H8A 0.4949 0.8335 0.8444 0.066*
H8B 0.3473 0.8016 0.8392 0.066*
H8C 0.3998 0.8801 0.7527 0.066*
C9 0.2855 (2) 0.5375 (3) 0.68386 (17) 0.0412 (7)
H9A 0.2537 0.6259 0.6423 0.062*
H9B 0.2239 0.5122 0.7246 0.062*
H9C 0.2992 0.4426 0.6470 0.062*
C10 0.4906 (2) 0.4488 (3) 0.84924 (16) 0.0327 (6)
C11 0.4060 (3) 0.4598 (3) 0.92525 (17) 0.0537 (8)
H11A 0.4329 0.3794 0.9733 0.081*
H11B 0.3184 0.4396 0.8978 0.081*
H11C 0.4131 0.5673 0.9529 0.081*
C12 0.4852 (3) 0.2784 (3) 0.80998 (19) 0.0501 (8)
H12A 0.5357 0.2727 0.7598 0.075*
H12B 0.3977 0.2505 0.7858 0.075*
H12C 0.5186 0.2028 0.8591 0.075*
C13 0.6274 (2) 0.4848 (3) 0.89552 (17) 0.0515 (8)
H13A 0.6519 0.4094 0.9467 0.077*
H13B 0.6325 0.5950 0.9194 0.077*
H13C 0.6842 0.4727 0.8496 0.077*
C14 0.8129 (2) 0.4543 (3) 0.51520 (17) 0.0299 (6)
C15 0.9983 (3) 0.3166 (3) 0.49216 (19) 0.0448 (7)
H15A 0.9561 0.2119 0.4853 0.067*
H15B 1.0858 0.3022 0.5216 0.067*
H15C 0.9964 0.3656 0.4309 0.067*
C16 1.0379 (2) 0.7499 (3) 0.86556 (17) 0.0409 (7)
H16A 0.9843 0.6549 0.8664 0.061*
H16B 1.0847 0.7684 0.9278 0.061*
H16C 1.0973 0.7324 0.8220 0.061*
C17 0.8227 (2) 0.9581 (3) 0.90962 (15) 0.0384 (7)
H17A 0.7633 1.0430 0.8857 0.058*
H17B 0.8674 0.9893 0.9707 0.058*
H17C 0.7768 0.8578 0.9151 0.058*
C18 1.0368 (2) 1.1119 (3) 0.81908 (16) 0.0314 (6)
C19 1.1006 (2) 1.1013 (3) 0.73279 (15) 0.0429 (7)
H19A 1.1597 1.1908 0.7326 0.064*
H19B 1.0367 1.1069 0.6771 0.064*
H19C 1.1462 0.9993 0.7333 0.064*
C20 1.1383 (2) 1.1213 (4) 0.90549 (17) 0.0510 (8)
H20A 1.1989 1.0339 0.9039 0.076*
H20B 1.0988 1.1113 0.9613 0.076*
H20C 1.1820 1.2248 0.9064 0.076*
C21 0.9558 (3) 1.2647 (3) 0.8138 (2) 0.0521 (9)
H21A 0.9137 1.2710 0.8685 0.078*
H21B 0.8924 1.2613 0.7577 0.078*
H21C 1.0095 1.3593 0.8116 0.078*