Table 1.
Data collection statistics
| Parameter | Value or description |
|---|---|
| Wavelength (Å) | 1.1159 |
| Space group | P1 |
| Cell dimensions (Å) | a = 48.5, b = 53.2, c = 69.0 |
| Cell angles (°) | α = 106.1, β = 93.3, γ = 104.4 |
| Resolution range (Å) | 30.00–3.0 (3.16–3.00) |
| Rmerge (%)a | 12.2 (44.6) |
| I/σ (I)a | 7.1 (2.4) |
| Completeness (%)a | 93.9 (94.7) |
| Redundancy | 3.0 (3.0) |
| Model refinement statistics | |
| No. of reflections (work/test) | 11,374/579 |
| Rwork/Rfree (%) | 21.4/28.8 |
| RMS deviation bond length (Å) | 0.010 |
| RMS deviation angle (°) | 1.506 |
| Avg temp (B) factor (Å2) | 50.6 |
| Ramachandran plot statistics | |
| Most favored regions (%) | 92.1 |
| Additional allowed regions (%) | 7.7 |
| Disallowed regions (%) | 0.2 |
a
Statistics for the outer resolution shell are shown in parentheses.