Table 2.
Compound | ESI | Time segment (min) | m/z parent ion | m/z daughter ion | Collision energy (eV) | Fragmentation amplitude (V) | Calibration curves | |
---|---|---|---|---|---|---|---|---|
Equation, n a | R 2 | |||||||
AMP | + | 1.86–3.48 | 350 | 160 | 20 | 90 | y = 410x − 30, 3 | 0.998 |
CIP | + | 7.33–12.58 | 332 | 314 | 20 | 110 | y = 927x + 2640, 3 | 0.993 |
ENR | + | 6.69–13.33 | 360 | 316 | 20 | 90 | y = 211x + 1437, 3 | 0.999 |
OTC | + | 1.49–12.87 | 461 | 426 | 20 | 90 | y = 78x + 71, 3 | 0.998 |
TYL | + | 2.80–11.87 | 916 | 174 | 35 | 110 | y = 709x + 697, 3 | 0.998 |
aNumber of concentrations for plotting calibration curves.