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. 2013 Apr 11;2013:351528. doi: 10.1155/2013/351528

Table 2.

Optimal conditions for the analysis of selected antibiotics and related calibration curves.

Compound ESI Time segment (min) m/z parent ion m/z daughter ion   Collision energy (eV) Fragmentation amplitude (V) Calibration curves
Equation, n a R 2
AMP + 1.86–3.48 350 160 20 90 y = 410x − 30, 3 0.998
CIP + 7.33–12.58 332 314 20 110 y = 927x + 2640, 3 0.993
ENR + 6.69–13.33 360 316 20 90 y = 211x + 1437, 3 0.999
OTC + 1.49–12.87 461 426 20 90 y = 78x + 71, 3 0.998
TYL + 2.80–11.87 916 174 35 110 y = 709x + 697, 3 0.998

aNumber of concentrations for plotting calibration curves.