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. 2013 May 21;8(5):e62225. doi: 10.1371/journal.pone.0062225

Table 7. Detection limit of the EPR signal for commercial composites, expressed as the time period needed for disappearance of the signal under the measurements conditions.

Commercial composites X-band detection threshold L-band detection threshold
Filtek Supreme Ultra 5 months 16 days
Venus Diamond 5 months 1 day
IPS Empress Direct 2 months* 4 days
Tetric EvoCeram 2 months* 2 days
Amaris 2 months 0 day
GrandioSo 2 months* 1 day
Gradia Direct X 3 months 1 day
GC Kalore 2 months 1 day
Ice 3 months 8 days
N'Durance 17 days 3 days
Clearfil AP-X >6 months 18 days
Clearfil Majesty Esthetic 3 months 8 days
Synergy D6 2 months 1 day
Esthet-X HD 2 months 3 days
TPH3 3 months 4 days
Ceram-X 2 months* 10 days
Artiste Nano 2 months 4 days
Simile 2 months 3 days
Herculite Ultra 18 days 2 days

The mass of the sample was 30 mg, a typical medium size restoration on an incisor.

*

detection threshold for the nine-lines signal. See table 8 for nitroxide-like signal threshold.