TABLE 1.
Crystallographic statistics for τ55-HPD
| τ55-HPD |
||
|---|---|---|
| Native | Mercury-derivative | |
| Data collection | ||
| Space group | P21212 | P21212 |
| Cell dimensions | ||
| a, b, c (Å) | 80.6, 86.7, 44.3 | 80.5, 86.6, 44.4 |
| Wavelength (Å) | 1.00849 | 1.00514 |
| Resolution (Å) | 50.0-1.50 (1.54-1.50) | 50.0-1.95 (2.00-1.95) |
| Rsym (%) | 16.1 (98.7) | 17.4 (81.3) |
| <I/σ(I)> | 15.5 (2.19) | 14.05 (2.27) |
| Completeness (%) | 99.5 (99.9) | 99.9 (99.6) |
| Multiplicity | 4.05 (4.02) | 4.24 (3.44) |
| Refinement | ||
| Resolution (Å) | 43.4-1.50 | |
| No. reflections | 50,251 | |
| Rwork/Rfree (%) | 15.6/18.3 | |
| No. atoms | ||
| Protein | 2,083 | |
| Other | 5 | |
| Water | 293 | |
| B-factor (Å2) | ||
| Protein | 18.7 | |
| Other | 32.1 | |
| Water | 12.9 | |
| RMSD | ||
| Bond lengths (Å) | 0.01 | |
| Bond angles (°) | 1.248 | |