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13C-1H dipolar coupling values of DMPC in magnetically-aligned 3:1 DMPC:DHPC bicelles with and without rat-IAPP20-29 using 2D PDLF solid-state NMR experiments at 37 °C. (A) Sample 1H-13C dipolar coupling spectral slices extracted from the 2D PDLF spectrum of bicelles containing 2% rat-IAPP20-29. (B) Dipolar coupling values calculated from the 2D PDLF experiment. Carbons 4-11 are poorly resolved and therefore represented as a single average value. (C) Labeling scheme for DMPC.
