Table 2.
CCS values for LE:Aβ1-40 Complexes Measured by IM-MS
Complex | m/z | CCS (Å2) | σ * |
---|---|---|---|
LE+ | 557.0 | 165 | 0.22 |
Aβ1-404+ | 1083.5 | 622 | 13.2 |
Aβ1-404+ | 1083.5 | 678 | 0.29 |
Aβ1-403+ | 1444.3 | 594 | 0.38 |
[Aβ1-40 + LE]3+ | 1629.6 | 638 | 0.84 |
[Aβ1-40 + LE2]3+ | 1815.0 | 683 | 0.43 |
[Aβ1-40 + LE3]3+ | 2000.3 | 731 | 0.18 |
Aβ1-40 Dimer5+ | 1733.0 | 946 | 12.7 |
[Aβ1-40 Dimer + LE]5+ | 1844.2 | 982 | 0.21 |
[Aβ1-40 Dimer + LE2]5+ | 1955.4 | 1032 | 1.54 |
[Aβ1-40 Dimer + LE3]5+ | 2066.6 | 1060 | 22.6 |
Standard deviations from measurements in triplicate. For real errors, including those from IM calibration, an additional ~3% must be added to these values.