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. 2013 Mar 13;14(2):558–568. doi: 10.1208/s12249-013-9940-6

Table III.

Comparison of the DSC and TGA Data of 10-DAB III and its Solid Forms

Compound Endotherm (°C)a ΔH (J/g) Endotherm (°C)b ΔH (J/g) Weight loss (%)
Experimental Expected
10-DAB III 247.97 54.51
Form I 129.86 35.54 246.01 50.99 12.84 12.54
Form II 138.60 102.80 252.67 56.33 12.92 13.80
Form III 166.05 93.77 248.20 57.20 21.60 22.28
Form IV 115.70 102.40 249.36 57.29 11.46 11.83

aEndotherms correspond to loss of solvent

bEndotherms correspond to onset temperature of solid forms