Table V.

SS NMR¹³C Chemical Shifts (δ/ppm) for 10-DAB III, Forms I to IV and Solution State of 10-DAB III

Carbon atom	Solution state	Solid state
	10-DAB III	10-DAB III	I	II	III	IV
1	77.31	76.80	78.76	76.77	78.08	79.15
2	75.23	75.41	76.64	75.48	76.87	76.36
3	46.90	46.46	47.21	46.33	47.21	47.17
4	80.47	80.63	80.49	80.59	80.33	80.83
5	84.13	82.83	86.49	83.01	83.87	86.54
6	39.84	38.59	39.33	38.85	39.27	40.57
7	71.29	71.40	71.73	70.70	70.30	71.93
8	57.42	57.86	57.12	58.06	58.27	57.50
9	210.68	211.72	210.15	214.36	215.53	210.38
10	74.74	73.12	75.14	73.05	74.42	75.54
11	134.86	132.83	133.48	134.83	134.93	131.99
12	141.92	147.58	143.83	144.55	140.98	143.74
13	66.44	65.85	66.02	65.90	67.69	66.85
14	36.94	36.97	36.96	36.98	37.03	37.07
15	42.83	42.76	42.64	43.10	43.12	43.19
16	20.53	18.90	17.86	18.65	20.80	18.56
17	27.13	25.91	26.63	25.94	28.88	26.28
18	15.15	15.49	15.58	15.61	15.04	14.72
19	10.07	10.60	9.63	10.78	10.58	10.05
20	75.84	75.41	75.14	75.48	78.08	77.26
21	169.88	172.43	172.45	172.17	171.90	173.03
22	22.66	21.70	20.94	21.92	25.67	20.49
23	165.61	164.85	167.61	164.88	167.36	168.09
24	130.69	129.48	127.46	127.13	130.47	128.53
25	129.87	128.14	134.84	129.36	134.93	134.29
29			132.64	128.79
26	129.01	127.12	131.86	128.47	132.87	129.88
28			129.67	127.95
27	133.53	131.97	130.22	132.74		129.88