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. 2013 Apr 12;21(1):31. doi: 10.1186/2008-2231-21-31

Scheme 2.

Scheme 2

Synthesis of aldehyde intermediates 7–9 and 11.Reagents and conditions: (a) Cl2 , CH3COOH; (b) R2OCOCH2Br, K2CO3, CH3COCH2CH3; (c) methyl iodide, K2CO3, DMF.