Table 3.
Bond angles [°] for 1.
| C(8)-O(7)-C(5) | 113.8(2) | N(12)-C(13)-N(14) | 124.97(19) |
| C(8)-O(7)-C(6) | 116.5(4) | N(12)-C(13)-N(15) | 113.37(18) |
| C(5)-O(7)-C(6) | 39.8(4) | N(14)-C(13)-N(15) | 121.60(18) |
| C(13)-N(14)-H(14A) | 121.2(16) | C(10)-C(9)-C(8) | 120.5(2) |
| C(13)-N(14)-H(14B) | 117.0(17) | O(7)-C(8)-C(2) | 122.1(2) |
| C(13)-N(15)-C(1) | 106.39(16) | O(7)-C(8)-C(9) | 115.08(19) |
| C(13)-N(15)-C(16) | 123.76(17) | C(2)-C(8)-C(9) | 122.8(2) |
| C(1)-N(15)-C(16) | 128.11(16) | C(2)-C(3)-C(4) | 113.01(19) |
| C(2)-C(1)-N(15) | 132.33(19) | C(6)-C(4)-C(22) | 123.2(5) |
| C(2)-C(1)-C(11) | 122.89(19) | C(6)-C(4)-C(5) | 42.8(5) |
| N(15)-C(1)-C(11) | 104.68(17) | C(22)-C(4)-C(5) | 116.2(3) |
| C(13)-N(12)-C(11) | 104.93(16) | C(6)-C(4)-C(3) | 125.8(5) |
| C(10)-C(11)-N(12) | 129.27(19) | C(22)-C(4)-C(3) | 110.8(2) |
| C(10)-C(11)-C(1) | 120.1(2) | C(5)-C(4)-C(3) | 109.9(2) |
| N(12)-C(11)-C(1) | 110.61(17) | C(6)-C(4)-C(23) | 116.2(7) |
| C(1)-C(2)-C(8) | 114.9(2) | C(5)-C(4)-C(23) | 131.1(5) |
| C(1)-C(2)-C(3) | 124.47(18) | C(3)-C(4)-C(23) | 114.0(5) |
| C(8)-C(2)-C(3) | 120.5(2) | O(7)-C(5)-C(4) | 113.6(3) |
| C(9)-C(10)-C(11) | 118.6(2) | C(4)-C(6)-O(7) | 113.0(8) |