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. 2013 May 31;9:1051–1072. doi: 10.3762/bjoc.9.118

Figure 23.

Figure 23

In-line solvent switching apparatus. The reactor output is directed into a bottle positioned on a hotplate. A flow of nitrogen gas removed the heated DCM solvent leaving the desired intermediate in DMF (a less volatile solvent). A webcam is directed at the evaporation setup so that it can be monitored remotely.