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This is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Two-step synthesis of branched aldehydes from aryl iodides using two reactive gases. A liquid–liquid extraction in between the two steps removes the salts and excess base before the second step.