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letter
. 2013 Apr 23;9:786–790. doi: 10.3762/bjoc.9.89

Table 1.

Optimization of reaction conditions for the synthesis of dye 1.

Entry Oxidant Base Yield, %a

1 p-chloranil Et3N 29
2 DDQ Et3N 7
3 Ce(NH4)2(NO3)6 Et3N 0
4 Ce(NH4)2(NO3)6 DBU 8
5 p-chloranil DBU 24b
6 p-chloranil K2CO3 0
7 p-chloranil NaOH 0

aIsolated yield, after column chromatography; byields varied from 8 to 24%.