Bruker X8 APEXII area-detector diffractometer | 6371 independent reflections |
Radiation source: fine-focus sealed tube | 3830 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.044 |
φ and ω scans | θmax = 31.4°, θmin = 2.5° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −14→14 |
Tmin = 0.739, Tmax = 0.867 | k = −10→10 |
29996 measured reflections | l = −39→39 |