Bruker SMART APEXII CCD diffractometer | 3130 independent reflections |
Radiation source: fine-focus sealed tube | 2053 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.047 |
ω and φ scans | θmax = 26.0°, θmin = 2.2° |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −10→10 |
Tmin = 0.464, Tmax = 0.523 | k = −12→13 |
12198 measured reflections | l = −19→22 |