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. 2013 May 22;69(Pt 6):o931–o932. doi: 10.1107/S1600536813012774
Bruker SMART APEXII CCD diffractometer 3130 independent reflections
Radiation source: fine-focus sealed tube 2053 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.047
ω and φ scans θmax = 26.0°, θmin = 2.2°
Absorption correction: multi-scan (SADABS; Bruker, 2008) h = −10→10
Tmin = 0.464, Tmax = 0.523 k = −12→13
12198 measured reflections l = −19→22