Bruker Kappa APEXII CCD diffractometer | 2982 independent reflections |
Radiation source: fine-focus sealed tube | 2560 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.020 |
ω and φ scans | θmax = 28.9°, θmin = 2.8° |
Absorption correction: multi-scan (SADABS; Sheldrick, 2004) | h = −8→8 |
Tmin = 0.970, Tmax = 0.985 | k = −26→34 |
5817 measured reflections | l = −10→9 |