Table 1. Hydrogen-bond geometry (Å, °).
D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
---|---|---|---|---|
N1—H1A⋯O10 | 0.89 | 2.19 | 2.909 (3) | 138 |
N1—H1A⋯O12 | 0.89 | 2.11 | 2.841 (4) | 139 |
N1—H1B⋯O18W | 0.89 | 1.85 | 2.700 (5) | 158 |
N1—H1C⋯O15i | 0.89 | 2.16 | 3.007 (4) | 159 |
N2—H2B⋯O10 | 0.91 (5) | 1.86 (5) | 2.709 (4) | 154 (4) |
N2—H2B⋯O16 | 0.91 (5) | 2.49 (4) | 3.125 (4) | 128 (3) |
N3—H3⋯O9ii | 0.86 | 2.56 | 2.992 (5) | 112 |
N3—H3⋯O14ii | 0.86 | 2.25 | 3.077 (4) | 160 |
O2—H2⋯O3iii | 0.82 | 1.86 | 2.657 (3) | 165 |
O17W—H17A⋯O5iv | 0.84 (2) | 2.27 (3) | 3.082 (4) | 162 (9) |
O17W—H17B⋯O3 | 0.84 (2) | 2.14 (8) | 2.864 (4) | 144 (12) |
O18W—H18A⋯O17W v | 0.83 (2) | 1.83 (2) | 2.664 (5) | 176 (5) |
O18W—H18B⋯O7 | 0.83 (2) | 2.32 (4) | 3.005 (5) | 140 (6) |
C3—H3B⋯O10 | 0.97 | 2.59 | 3.210 (4) | 122 |
C9—H9⋯O8vi | 0.93 | 2.40 | 3.177 (4) | 141 |
C17—H17⋯O11iv | 0.93 | 2.36 | 3.177 (3) | 147 |
Symmetry codes: (i) ; (ii) ; (iii) ; (iv) ; (v) ; (vi) .