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Decarboxylative palladation as monitored by 1H NMR spectroscopy (Substrate = 9). Reaction conditions: initial concentration [6] = 0.09 M and [Pd(O2CCF3)2] = 0.11 M, 0.75 mL DMSO-d6, 70 °C. Equation of the line for b is y = −2.499x – 2.641. R2 = 0.964.
