Table 2.
Yield are reported as a combination of isomers and reaction performed on 0.5 mmol scale. Enatioselectivity determined SFC equipped with a chiral column.
Ratio of γ to β–product as detemined by either 1H NMR or gas chromatography.
Enatioselectivity of the β-product is 99:1 er.
Reaction performed on 10 mmol scale.