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letter
. 2013 Jun 13;9:1141–1147. doi: 10.3762/bjoc.9.127

Table 3.

The yield of diphenyl selenide 3aa upon changing the ratio 1a/2a.

graphic file with name Beilstein_J_Org_Chem-09-1141-i033.jpg

entry amount of 1a amount of 2a yield of 3aaa

1 0.1 mmol 0.5 mmol 69%
0.138 mmol
2 0.1 mmol 0.3 mmol 69%
0.138 mmol
3 0.1 mmol 0.1 mmol 59%
0.118 mmol
4 0.1 mmol 0.067 mmol
(2/3 equiv)
57%
0.118 mmol
5 0.2 mmol 0.1 mmol 88%b
0.263 mmol

aThe yields were determined by HPLC based on the amount of 1a. bThe yield was calculated based on the amount of 2a.