Table 4. Crystallographic data and refinement statistics.
| Data collection | |
| Space group | P21212 |
| Unit cell lengths (Ål) | a = 66.7, b = 164.6, c = 90.6 |
| Resolution (Ål) | 20–3.2 |
| Rmergea | 11.5 (58.7) b |
| % completenessa | 97.1 (90.4) b |
| I/sigma (I) averagea | 20.13 (4.14) b |
| No. of unique reflectionsa | 16636 (685) b |
| Redundancya | 15.5 (16.1) b |
| Refinement | |
| Resolution (Ål) | 20–3.2 |
| R work | 0.208 (0.259) c |
| R free | 0.269 (0.349) c |
| Root mean square deviation χ2 bonds (Å) | 0.006 |
| Root mean square deviation χ2 angles (°) | 1.16 |
| Residues in Ramachandran favoured region d | 670 (91.9%) |
| Residues in Ramachandran allowed region d | 39 (5.3%) |
| Residues in Ramachandran outlier region d | 20 (2.7%) |
a
Statistics on a merged dataset resulting from 4 crystals collected at ID14-eh2, ID29, ID14-eh1, BM14, ESRF, Grenoble.
b
Statistics for the high-resolution bin (3.25–3.20 Å) are in parentheses.
c
Statistics for the high-resolution bin (3.28–3.20 Å) are in parentheses.
d
Including prolines and glycines – Statistics provided by RAMPAGE [65].