Table 1.
Position | 1 | |
---|---|---|
δC | δH (J/Hz) | |
1 | 193.4 | 10.21 (1H, s) |
2 | 112.9 | |
3 | 163.6 | |
4 | 102.1 | 6.20 (1H, s) |
5 | 158.5 | |
6 | 120.0 | |
7 | 148.5 | |
8 | 38.7 | 4.71 (1H, d, 6.0) |
9 | 121.4 | |
10 | 150.0 | |
11 | 114.0 | |
12 | 135.6 | |
13 | 119.4 | |
14 | 154.0 | |
15 | 17.9 | 2.42 (3H, s) |
16 | 60.2 | 3.59 (3H, s) |
1′ | 27.5 | 2.81 (2H, overlapped) |
2′ | 51.1 | 2.81 (1H, overlapped) |
3′ | 75.6 | |
4′ | 26.8 | 1.55 (3H, s) |
5′ | 24.6 | 1.38 (3H, s) |
OH-3 | 11.74, brs |
a Measured at 400 MHz (1H) and 100 MHz (13C), CDCl3.