Table 1.
No. carbon | δH, J in Hz | δCa |
---|---|---|
2 | 167.9 s | |
3 | 5.14 (1H, s) | 87.8 d |
4 | 170.9 s | |
5 | 129.1 s | |
6 | 143.9 s | |
7 | 124.4 s | |
8 | 6.85 (1H, d, 1.6) | 110.2 d |
9 | 147.6 s | |
10 | 149.4 s | |
11 | 6.82 (1H, d, 8.0) | 108.1 d |
12 | 6.92 (1H, dd, 8.0, 1.6) | 125.1 d |
13 | 6.04 (2H, s) | 101.7 t |
4-OCH3b | 3.76 (3H, s) | 59.1 q |
6-OCH3b | 3.67 (3H, s) | 59.0 q |
multiplicitiy obtained from DEPT-135 and DEPT-90 spectra, s: C; d: CH; t: CH2; q: CH3;
Signals interchangeable