Table 3.
Selected bond distances (Å) and angles (°) for H-bonding interactions in the solid-state structure of 1.
| Donor Atom (D) | Hydrogen Atom (H) | Acceptor Atom (A) | Distance D-H | Distance H-A | Distance D-A | Bond Angle DHA |
|---|---|---|---|---|---|---|
| O1 | H1W1 | O6 | 0.82(2) | 1.95(2) | 2.759(3) | 174(4) |
| O1 | H1W2 | O10 | 0.84(2) | 1.99(3) | 2.793(3) | 160(4) |
| O1 | H1W2 | O10′ | 0.84(2) | 1.94(2) | 2.77(2) | 174(4) |
| O2 | H2W1 | O9 | 0.85(2) | 1.90(2) | 2.745(6) | 171(3) |
| O2 | H2W1 | O9′ | 0.85(2) | 1.81(3) | 2.636(19) | 163(4) |
| O2 | H2W2 | O5 | 0.79(2) | 2.01(2) | 2.789(3) | 171(4) |
| O3 | H3W1 | O4 | 0.82(2) | 2.07(3) | 2.864(3) | 157(3) |
| O3 | H3W2 | O11 | 0.84(2) | 1.87(3) | 2.702(4) | 170(4) |
| N4 | H4A | O7 | 0.93 | 1.90 | 2.755(6) | 152 |