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. Author manuscript; available in PMC: 2014 Jun 24.
Published in final edited form as: Tetrahedron. 2013 Apr 15;69(25):5205–5220. doi: 10.1016/j.tet.2013.04.041

Scheme 10.

Scheme 10

Representative bromine installation studies. Reagents and conditions: a) ClCH2SO2Cl, pyr, DMAP; b) LiBr, DMPU; c) HBr, AcOH or PBr3, SiO2.