. 2013 May 29;11(6):1853–1865. doi: 10.3390/md11061853

Table 2.

¹H and ¹³C NMR spectroscopic data of 4–6.

Position		4		5		6
Position		δ_H (J in Hz) ^a	δ_C (mult.) ^b	δ_H (J in Hz) ^c	δ_C (mult.) ^d	δ_H (J in Hz) ^c	δ_C (mult.) ^d
1	α	0.91 m	31.9, CH₂^e	0.93 m	31.0, CH₂		165.4, C
	β	2.23 m		2.40 dt (14.0, 4.0)
2	α	1.83 m	29.3, CH₂	1.40 m	30.3, CH₂	5.81 s	116.6, CH
	β	1.44 m		1.87 m
3		3.53 m	76.7, CH	3.50 m	76.7, CH		157.0, C
4	α	1.62 m	34.4, CH₂	1.71 m	35.9, CH₂	2.22 d (4.4) ^f	35.0, CH₂
	β	1.33 m		1.23 m		2.27 m
5		1.25 m	44.8, CH	1.36 m	43.3, CH	4.46 m	75.7, CH
6	α	1.27 m	28.3, CH₂	1.53 m	28.3, CH₂	1.99 s	23.0, CH₃
	β			1.91 m
7	α	0.92 m	32.0, CH₂	1.07 m	32.0, CH₂
	β	1.75 m		1.90 m
8		1.50 m	35.9, CH	1.43 m	37.0, CH
9		0.75 m	54.5, CH	0.95 m	52.8, CH
10			38.1, C		51.8, C
11	α	1.65 m	21.8, CH₂	1.26 m	21.4, CH₂
	β	1.35 m		1.69 m
12	α	0.97 m	37.8, CH₂	0.98 m	37.3, CH₂
	β	1.68 m		1.66 m
13			43.6, C		43.4, C
14		1.02 m	55.9, CH	0.93 m	55.7, CH
15	α	1.68 m	24.7, CH₂	1.14 m	24.6, CH₂
	β	1.18 m		1.66 m
16	α	1.79 m	27.2, CH₂	1.50 m	27.1, CH₂
	β	1.56 m		1.76 m
17		1.95 dt (18.0,8.0) ^f	55.3, CH	1.93 m	55.3, CH
18		0.57 s	13.0, CH₃	0.52 s	12.8, CH₃
19		4.20 d (12.0)	62.8, CH₂	10.0 s	208.5, CH
		4.34 d (12.0)
20		5.74 ddd (18.0, 10.0, 8.0)	139.8, CH	5.72 ddd (18.0, 10.0, 8.0)	139.5, CH
21		4.95 br d (18.0)	114.5, CH₂	4.96 br d (18.0)	114.7, CH₂
		4.96 br d (10.0)		4.97 br d (10.0)
1′		5.13 d (4.0)	94.6, CH	5.12 d (3.6)	94.8, CH	1.52 m	42.3, CH₂
						1.68 m
2′		4.86 dd (10.5, 4.0)	72.0, CH	4.84 dd (10.0, 3.6)	72.0, CH	2.66 m	28.9, CH
3′		4.00 dd (10.5, 3.5)	68.6, CH	3.98 dd (10.0, 3.2)	68.5, CH	1.34 m	36.9, CH₂
4′		3.81 d (3.5)	72.3, CH	3.80 d (3.2)	72.3, CH	1.20 m	24.2, CH₂
						1.34 m
5′		4.09 q (6.5)	65.3, CH	4.06 q (6.8)	65.4, CH	1.08 m	37.2, CH₂
6′		1.28 d (6.5)	16.1, CH₃	1.27 d (6.8)	16.1, CH₃	1.38 m	32.7, CH
7′						1.08 m	37.3, CH₂
						1.26 m
8′						1.24 m	21.3, CH₂
9′						1.70 m	41.0, CH₂
10′							82.5, C
11′						1.42 s	26.1, CH₃
12′						1.42 s	26.1, CH₃
13′						0.85 d (6.4)	19.6, CH₃
14′						0.93 d (6.0)	19.9, CH₃
OAc		2.06 s	21.1, CH₃	2.12 s	21.1, CH₃	1.97 s	22.5, CH₃
		2.13 s	21.2, CH₃		171.5, C		170.5, C
			171.3, C
			171.5, C

^a Spectra recorded at 500 MHz in CDCl₃; ^b Spectra recorded at 125 MHz in CDCl₃; ^c Spectra recorded at 400 MHz in CDCl₃; ^d Spectra recorded at 100 MHz in CDCl₃; ^e Deduced from DEPT; ^f J values (Hz) in parentheses.