Table 1.
No. | δC | δH ( J in Hz) | No. | δC | δH ( J in Hz) |
---|---|---|---|---|---|
1 | 162.5, C | 9 | 60.1, CH2 | 3.40, m | |
2-NH | 8.62, d (2.8) | 10 | 118.1, CH | 6.97, s | |
3 | 55.0, CH | 3.94, m | 11 | 34.5, CH3 | 2.73, s |
4 | 167.9, C | 1′ | 133.8, C | ||
6 | 132.4, C | 2′/6′ | 129.2, CH | 7.42, d (7.5) | |
7 | 30.6, CH2 | a 1.79, m | 3′/5′ | 128.3, CH | 7.30, t (7.5) |
b 1.71, m | 4′ | 128.1, CH | 7.34, t (7.5) | ||
8 | 28.0, CH2 | 1.51, m | OH | 4.48, br s |
a Measured at 500 MHz for 1H and 125 MHz for 13C.