. Author manuscript; available in PMC: 2014 Aug 15.

Published in final edited form as: Bioorg Med Chem. 2013 Mar 7;21(16):4778–4785. doi: 10.1016/j.bmc.2013.02.040

Table 1.

HPLC retention times (RT) and HRMS data of Tn-, STn-, T-, and ST-MUC1 glycopeptides synthesized.

Glycopeptides	RT (min)	Exact Mass (m/z)	Observed Mass (m/z)
2	15.87	1257.5568^a	1257.5649^a
3	10.85	1546.6377^b	1546.6521^b
4	11.42	1571.6442^b	1571.6598^b
5	10.29	1562.6326^b	1562.6472^b
6	10.53	1587.6391^b	1587.6539^b
7	13.57	1419.6097^a	1419.6118^a
8	8.90	1708.6905^b	1708.7031^b
9	9.57	1733.6970^b	1733.7067^b
10	8.71	1724.6855^b	1724.6964^b
11	9.37	1749.6919^b	1749.7059^b

The masses given are for ^a[M + H] (positive mode) or ^b[M − H] (negative mode).