Table 1. Crystallographic statistics.
Data collection | |
Space group | P43212 |
a, b, c (Å) | 83.00, 83.00, 175.26 |
Resolution (Å) | 29.4–3.04 (3.25–3.04) |
Rmerge | 0.111 (0.868)a |
<I/σ(I)> | 15.2 (2.9) |
CC1/2 b | 0.999 (0.929) |
Completeness (%) | 99.2 (96.5) |
Multiplicity | 13.4 (11.7) |
Wilson B-factor (Å2) | 79.3 |
Refinement | |
Resolution (Å) | 29.4–3.04 |
Reflections | 12287 |
Protein atoms | 3153 |
Solvent atoms or molecules | 2 Mg2+, 1 Cl–, 1 bis-Tris |
Rwork | 0.246 |
Rfree | 0.298 |
R.m.s. deviation bonds (Å) | 0.003 |
R.m.s. deviation angles (°) | 0.65 |
Average atomic B-factor (Å2) | 83.9 |
Ramachandran plot (%)c | 94.8, 4.9, 0.3 |