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. 2013 Jul 20;69(Pt 8):1617–1632. doi: 10.1107/S0907444913012274

Table 6. Final statistics for structures related to group A and group B of ultralente insulin.

The values in parentheses are for the high-resolution data range.

  Group A Group B
Resolution range (Å) 24.36–2.10 (2.21–2.10) 24.32–2.00 (2.11–2.00)
R merge 0.138 (0.799) 0.185 (0.584)
R meas 0.153 (0.888) 0.203 (0.658)
R p.i.m. 0.065 (0.382) 0.085 (0.289)
I/σ(I)〉 7.4 (2.3) 7.4 (2.8)
Multiplicity 5.1 (5.1) 5.1 (5.1)
Completeness (%) 99.9 (100.0) 99.5 (100.0)
No. of reflections 24303 28373
No. of unique reflections 4775 5551
R work/R free (%) 18.5/24.8 20.9/28.0
R.m.s.d., bonds (Å) 0.016 0.015
R.m.s.d., angles (°) 1.923 1.877
Unit-cell parameters (Å)
a 80.05 81.02
c 34.25 33.75