Table 6. Final statistics for structures related to group A and group B of ultralente insulin.
The values in parentheses are for the high-resolution data range.
| Group A | Group B | |
|---|---|---|
| Resolution range (Å) | 24.36–2.10 (2.21–2.10) | 24.32–2.00 (2.11–2.00) |
| R merge | 0.138 (0.799) | 0.185 (0.584) |
| R meas | 0.153 (0.888) | 0.203 (0.658) |
| R p.i.m. | 0.065 (0.382) | 0.085 (0.289) |
| 〈I/σ(I)〉 | 7.4 (2.3) | 7.4 (2.8) |
| Multiplicity | 5.1 (5.1) | 5.1 (5.1) |
| Completeness (%) | 99.9 (100.0) | 99.5 (100.0) |
| No. of reflections | 24303 | 28373 |
| No. of unique reflections | 4775 | 5551 |
| R work/R free (%) | 18.5/24.8 | 20.9/28.0 |
| R.m.s.d., bonds (Å) | 0.016 | 0.015 |
| R.m.s.d., angles (°) | 1.923 | 1.877 |
| Unit-cell parameters (Å) | ||
| a | 80.05 | 81.02 |
| c | 34.25 | 33.75 |