Table 1.
Comp. No. | Ar | Melting point (°C) | Yield (%) | Mol. form. (Mol. wt.) |
---|---|---|---|---|
4 | 4-FC6H4 | 203–205 | 92 | C18H21FN2O (300.37) |
5 | 4-ClC6H4 | 211–212 | 90 | C18H21ClN2O (316.82) |
6 | 2-ClC6H4 | 262–265 | 90 | C18H21ClN2O (316.82) |
7 | 4-BrC6H4 | 234–235 | 95 | C18H21BrN2O (361.28) |
8 | 3-CH3C6H4 | 241–243 | 86 | C19H24N2O (296.41) |
9 | 2-NO2C6H4 | 217–219 | 89 | C18H21N3O3 (327.38) |
10 | 3-NO2C6H4 | 248–249 | 90 | C18H21N3O3 (327.38) |
11 | 4-NO2C6H4 | 231–234 | 94 | C18H21N3O3 (327.38) |
12 | 4-(Me2N)C6H4 | 152–156 | 87 | C20H27N3O (325.45) |
13 | 2,6-Cl2C6H3 | 256–259 | 87 | C18H20Cl2N2O (351.27) |
14 | 3,4-(CH3O)2C6H3 | 232–234 | 85 | C20H26N2O3 (342.43) |
15 | 2-Cl,5-FC6H3 | 262–265 | 90 | C18H20ClFN2O (334.82) |
16 | 2-Cl,5-NO2C6H3 | 223–225 | 85 | C18H20ClN3O3 (361.82) |
17 | 2-Thienyl | 270–272 | 90 | C16H20N2OS (288.41) |
18 | 4-FC6H4 | 149–151 | 90 | C20H23FN2O2S (374.47) |
19 | 4-ClC6H4 | 182–184 | 87 | C20H23ClN2O2S (390.93) |
20 | 2-ClC6H4 | 210–212 | 85 | C20H23ClN2O2S (390.93) |
21 | 4-BrC6H4 | 177–179 | 89 | C20H23BrN2O2S (435.38) |
22 | 3-CH3C6H4 | 186–188 | 86 | C21H26N2O2S (370.51) |
23 | 4-(Me2N)C6H4 | 112–114 | 84 | C22H29N3O2S (399.55) |
24 | 2,6-Cl2C6H3 | 195–197 | 85 | C20H22Cl2N2O2S (425.37) |
25 | 3,4-(CH3O)2C6H3 | 175–177 | 89 | C22H28N2O4S (416.53) |
26 | 2-Cl,5-FC6H3 | 185–187 | 82 | C20H22ClFN2O2S (408.92) |
27 | 2-Thienyl | 230–232 | 82 | C18H22N2O2S (362.51) |
28 | 4-FC6H4 | 85–89 | 49 | C20H23FN2O2 (342.41) |
29 | 2-ClC6H4 | 110–112 | 50 | C20H23ClN2O2 (358.86) |
30 | 2-NO2C6H4 | 128–131 | 39 | C20H23N3O4 (369.41) |
31 | 3-NO2C6H4 | 165–169 | 42 | C20H23N3O4 (369.41) |
32 | 4-NO2C6H4 | 195–197 | 47 | C20H23N3O4 (369.41) |
33 | 2-Cl,5-NO2C6H3 | 159–163 | 45 | C20H22ClN3O4 (403.86) |