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. Author manuscript; available in PMC: 2014 Sep 1.
Published in final edited form as: Bioorg Med Chem. 2013 Mar 5;21(17):5629–5646. doi: 10.1016/j.bmc.2013.02.016

Scheme 9.

Scheme 9

(a) TBDPSCl, imidazole; (b) BnOCOCl, NaHCO3; (c) HOAc/H2O/THF; (d) BzCl, py; (e) Me2CO, Me2C(OMe)2, TsOH; (f) NaOMe, MeOH; (g) (BnO)2PNiPr2, tetrazole, then MCPBA; (h) Bu4NF, THF; (i) TFA/THF/H2O; (j) H2, Pd black; (k) NaBH3CN, 8, Et3N, MeOH.