Scheme 2.
Synthesis of MitoDNP-SUM. a) iPrMgCl, LiCl, THF, −78 °C; b) −78 °C to RT; c) THF, LiCl, iPrMgCl, −78 °C; d) −78 °C to RT; e) 1-fluoro-2,4-dinitrobenzene, Et3N, acetone, 40 °C; f) HCl, MeOH/CH2Cl2, RT; g) Cs2CO3, MeCN, RT.
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