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. 2013 Jul 8;41(15):7566–7576. doi: 10.1093/nar/gkt488

Figure 3.

Figure 3.

The NOESY spectrum for the DDD-XY duplex, showing the assignments of the O6-Bn-dG and dPer protons. The cross-peaks in (a) are assigned as follows: 1a, T8 CH3→X4 Hmeta; 2a T8 CH3→X4 Hortho. The cross-peaks in (b) are assigned as follows:1b, T8 H2′→X4 Hmeta; 2b, T8 H2′′→X4 Hmeta; 3b, T8 H2′→X4 Hortho; 4b, T8 H2''→X4 Hortho; 5b, Y9 H2′/H2''→Y9 H8; 6b, Y9 H2′/H2′′→Y9 H9; 7b, C3 H2′→Y9 H6; 8b, Y9 H2′/H2′′→Y9 H1′. The cross-peaks in (c) are assigned as follows: 1c, X4 Hm1→X4 Hmeta; 2c, X4 Hm2→X4 Hmeta; 3c, Y9 H4′→X4 Hmeta; 4c, X4 Hm2→X4 Hpara; 5c, X4 Hm1→X4 Hortho; 6c, X4 Hm2→X4 Hortho; 7c, Y9 H4′→X4 Hortho; 8c, Y9 H4′ →Y9 H8; 9c, Y9 H3′→Y9 H9; 10c, Y9 H4′→Y9 H1′; 11c, Y9 H3′→Y9 H1′. The cross-peaks in (d) are assigned as follows: 1d, X4 Hortho→X4 Hmeta; 2d, X4 Hpara→X4 Hmeta; 3d, X4 Hortho→X4 Hpara; 4d, Y9 H1′→Y9 H8; 5d, Y9 H6→Y9 H8; 6d, Y9 H7→Y9 H8; 7d, Y9 H9→X4 Hortho; 8d, Y9 H9→Y9 H8; 9d, Y9 H4→Y9 H5; 10d, Y9 H6→Y9 H5; 11d, Y9 H7→Y9 H5; 12d, Y9 H1′→Y9 H9; 13d, Y9 H7→Y9 H9. The spectrum was collected at 10°C at 900 MHz, using a 250 ms mixing time.